X-ray diffraction cell for studying solid-gas reactions under gas pressures to 100 bar

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Title X-ray diffraction cell for studying solid-gas reactions under gas pressures to 100 bar
Author Gray, Evan; Cookson, D.J.; Blach, Tomasz Piotr
Journal Name Journal of Applied Crystallography
Editor Peter Strickland
Year Published 2006
Place of publication Denmark
Publisher Blackwell Munksgaard
Abstract A pressure cell designed for high-energy X-ray diffraction in transmission mode is described. The cell is intended for use at temperatures up to 573 K with samples that are large enough to permit the real-time determination of the amount of absorbed gas by measuring the gas pressure. The design is driven by the need to ensure that the sample temperature is constant and uniform, despite the heat flow accompanying the reaction between the gas and the sample. The use of the cell is illustrated by its application to elucidating the hydriding phase transformation in the LaNi5-H2 system.
Peer Reviewed Yes
Published Yes
Publisher URI http://journals.iucr.org/j/journalhomepage.html
Alternative URI http://dx.doi.org/10.1107/S0021889806039069
Volume 39
Page from 850
Page to 855
ISSN 0021-8898
Date Accessioned 2007-06-21
Date Available 2009-09-17T07:24:23Z
Language en_AU
Research Centre Queensland Micro and Nanotechnology Centre
Faculty Faculty of Science, Environment, Engineering and Technology
Subject PRE2009-Condensed Matter Physics-Structural Properties
URI http://hdl.handle.net/10072/14353
Publication Type Journal Articles (Refereed Article)
Publication Type Code c1

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